Study on Azo-aldehyde Part-X: Synthesis, Characterization, Liquid Chromatography and Biological screening of Azo-salicylaldehyde from Nitro and Methyl-anilines
C. J. Patil , S. M. Harimkar , S. V. Rajput
DOI : 10.46335/IJIES.2023.8.5.1
Abstract –Azo derivatives of salicylaldehyde (I-II) were prepared by reaction of Salicylaldehyde derivatives (Ic) with diazonium salt of variedly substituted aniline (Ia-b) by diazo couplingsequence (retention of N). These were characterized by Schiff reagent test, analytical (viz. colour, physical constant, TLC and HPLC) and spectral (viz. UV-Vis, FTIR) methods. A simple, fast and accurate method has been developed and reported for the identification and screening of Azo aldehydes by chromatographic method, High-performance liquid chromatography (HPLC) and also the biological potency studywere reported.
